Research Progress in the Electron Beam Additive Manufacturing for Fabricating Ni-based Superalloys

SUN Jing, WANG Jie, JIANG Xiao, WANG Chaoyue, YIN Ying, ZHANG Ying, YIN Yuhuan

Journal of Netshape Forming Engineering ›› 2026, Vol. 18 ›› Issue (6) : 151-170.

PDF(1805 KB)
PDF(1805 KB)
Journal of Netshape Forming Engineering ›› 2026, Vol. 18 ›› Issue (6) : 151-170. DOI: 10.3969/j.issn.1674-6457.2026.06.014
Additive Manufacturing

Research Progress in the Electron Beam Additive Manufacturing for Fabricating Ni-based Superalloys

  • SUN Jing*, WANG Jie, JIANG Xiao, WANG Chaoyue, YIN Ying, ZHANG Ying, YIN Yuhuan
Author information +
History +

Abstract

The EBM (electron beam additive manufacturing, EBM) manufacturing of Ni-based superalloys has a promising application prospect in the rapid manufacturing of engine parts. Based on a plenty of literature analysis, to address the cracking problem of nickel-based superalloys fabricated by EBM, the work aims to review the mechanism and impact factors for cracking from the perspectives of component microstructure evolution and elemental segregation behavior and conduct targeted research on crack suppression measures and their effects for EBM-fabricated nickel-based superalloy components in terms of post-heat treatment, microstructure optimization, and composition regulation. EBM-fabricated nickel-based superalloy components exhibited a prominent growth tendency of coarse columnar grains along the building height direction. Cracks mostly initiated at the γ/γ′ interfaces on columnar grain boundaries and rapidly propagated along high-angle grain boundaries. Obvious segregation of elements such as B, Hf and Zr was observed on both sides of the cracks. Further analysis revealed that a nano-amorphous layer existed at the interface between M2B metallic compounds and the γ′ phase, which fully verified that the cracks in additively manufactured nickel-based superalloy components were predominantly hot cracks. Then, HIP treatment could effectively decrease pores and micro-cracks, but the temperature must exceed the γ′ solvent temperature and thermal cracks would regenerate during the subsequent solution treatment process. Optimizing the scanning strategy or in-situ heat-treatment could promote the transformation of coarse columnar into equiaxed crystals, and additionally, composition regulation could effectively reduce the solidification temperature range, all of which had certain effects on suppressing hot cracking. The research results can further promote the application of EBM for nickel-based superalloys in the aerospace field.

Key words

Ni-based superalloy / electron beam additive manufacturing / microstructure evolution / cracking mechanism / heat treatment / failure mode

Cite this article

Download Citations
SUN Jing, WANG Jie, JIANG Xiao, WANG Chaoyue, YIN Ying, ZHANG Ying, YIN Yuhuan. Research Progress in the Electron Beam Additive Manufacturing for Fabricating Ni-based Superalloys[J]. Journal of Netshape Forming Engineering. 2026, 18(6): 151-170 https://doi.org/10.3969/j.issn.1674-6457.2026.06.014

References

[1] 陈忠兵, 梁振新, 齐铂金, 等. 超音频脉冲方波电弧对镍基合金焊缝金属高温低塑性裂纹(DDC)的影响[J]. 电焊机, 2025, 55(6): 58-64.
CHEN Z B, LIANG Z X, QI B J, et al.Influence of Ultra-High Frequency Pulsed Square Wave Arc on DDC of Nickel-Based Alloy Weld Metal[J]. Electric Welding Machine, 2025, 55(6): 58-64.
[2] 李洋, 徐睦忠, 刘自刚, 等. 镍基合金与不锈钢异种焊接接头全位置自动TIG焊接工艺研究[J]. 电焊机, 2025, 55(3): 82-87.
LI Y, XU M Z, LIU Z G, et al.Study on All-Position Automatic TIG Welding Technology for Dissimilar Joints of Nickel-Based Alloy and Stainless Steel[J]. Electric Welding Machine, 2025, 55(3): 82-87.
[3] 钱虎虓, 梁啸宇, 李阳, 等. 电子束粉床熔融制备镍基高温合金构件的研究进展[J]. 航空材料学报, 2024, 44(1): 46-58.
QIAN H X, LIANG X Y, LI Y, et al.Research Progress in Fabrication of Nickel-Based Superalloy Components by Electron Beam Powder Bed Fusion[J]. Journal of Aeronautical Materials, 2024, 44(1): 46-58.
[4] BEHERA B C, ALEMAYEHU H, GHOSH S, et al.A Comparative Study of Recent Lubri-Coolant Strategies for Turning of Ni-Based Superalloy[J]. Journal of Manufacturing Processes, 2017, 30: 541-552.
[5] AKHAVAN NIAKI F, MEARS L.A Comprehensive Study on the Effects of Tool Wear on Surface Roughness, Dimensional Integrity and Residual Stress in Turning IN718 Hard-to-Machine Alloy[J]. Journal of Manufacturing Processes, 2017, 30: 268-280.
[6] DE BARTOLOMEIS A, NEWMAN S T, JAWAHIR I S, et al.Future Research Directions in the Machining of Inconel 718[J]. Journal of Materials Processing Technology, 2021, 297: 117260.
[7] LIU H, ZHAO X B, YUAN Y, et al.Influence of Thermal Exposure on Microstructural Stability and Tensile Properties of a New Ni-Base Superalloy[J]. Journal of Materials Research and Technology, 2022, 21: 4462-4472.
[8] WANG X Q, GONG X B, CHOU K.Review on Powder-Bed Laser Additive Manufacturing of Inconel 718 Parts[J]. Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 2017, 231(11): 1890-1903.
[9] ZHAO Y N, GUO Q Y, MA Z Q, et al.Comparative Study on the Microstructure Evolution of Selective Laser Melted and Wrought IN718 Superalloy during Subsequent Heat Treatment Process and Its Effect on Mechanical Properties[J]. Materials Science and Engineering: A, 2020, 791: 139735.
[10] FENG Q S, WU Y, LI J K, et al.Effects of Intermediate Temperature on the Grain Boundary and γ' Precipitates of Nickel-Based Powder Superalloy under Interrupted Cooling[J]. Journal of Alloys and Compounds, 2022, 922: 166310.
[11] HOSSEINI E, POPOVICH V A.A Review of Mechanical Properties of Additively Manufactured Inconel 718[J]. Additive Manufacturing, 2019, 30: 100877.
[12] SHAHWAZ M, NATH P, SEN I.A Critical Review on the Microstructure and Mechanical Properties Correlation of Additively Manufactured Nickel-Based Superalloys[J]. Journal of Alloys and Compounds, 2022, 907: 164530.
[13] LEE D, PARK S, LEE C H, et al.Correlation between Microstructure and Mechanical Properties in Additively Manufactured Inconel 718 Superalloys with Low and High Electron Beam Currents[J]. Journal of Materials Research and Technology, 2024, 28: 2410-2419.
[14] SADEGHI E, KARIMI P, ESMAEILIZADEH R, et al.A State-of-the-Art Review on Fatigue Performance of Powder Bed Fusion-Built Alloy 718[J]. Progress in Materials Science, 2023, 133: 101066.
[15] SATYANARAYANA D V V, PRASAD N E. Nickel-Based Superalloys[M]. Singapore: Springer Singapore, 2016: 199-228.
[16] CHEN J B, CHEN J Y, WANG Q J, et al.Enhanced Creep Resistance Induced by Minor Ti Additions to a Second Generation Nickel-Based Single Crystal Superalloy[J]. Acta Materialia, 2022, 232: 117938.
[17] MACKAY R A, GABB T P, GARG A, et al.Influence of Composition on Microstructural Parameters of Single Crystal Nickel-Base Superalloys[J]. Materials Characterization, 2012, 70: 83-100.
[18] HAMDI H, ABEDI H R.Thermal Stability of Ni-Based Superalloys Fabricated through Additive Manufacturing: A Review[J]. Journal of Materials Research and Technology, 2024, 30: 4424-4476.
[19] CHANDRA S, TAN X P, NARAYAN R L, et al.A Generalised Hot Cracking Criterion for Nickel-Based Superalloys Additively Manufactured by Electron Beam Melting[J]. Additive Manufacturing, 2021, 37: 101633.
[20] SANCHEZ S, SMITH P, XU Z K, et al.Powder Bed Fusion of Nickel-Based Superalloys: A Review[J]. International Journal of Machine Tools and Manufacture, 2021, 165: 103729.
[21] XU J H, KONTIS P, PENG R L, et al.Modelling of Additive Manufacturability of Nickel-Based Superalloys for Laser Powder Bed Fusion[J]. Acta Materialia, 2022, 240: 118307.
[22] KÖRNER C. Additive Manufacturing of Metallic Components by Selective Electron Beam Melting—A Review[J]. International Materials Reviews, 2016, 61(5): 361-377.
[23] MURR L E.Metallurgy of Additive Manufacturing: Examples from Electron Beam Melting[J]. Additive Manufacturing, 2015, 5: 40-53.
[24] WANG N, MOKADEM S, RAPPAZ M, et al.Solidification Cracking of Superalloy Single- and Bi-Crystals[J]. Acta Materialia, 2004, 52(11): 3173-3182.
[25] CHEN Y, LU F G, ZHANG K, et al.Dendritic Microstructure and Hot Cracking of Laser Additive Manufactured Inconel 718 under Improved Base Cooling[J]. Journal of Alloys and Compounds, 2016, 670: 312-321.
[26] DUPONT J N, LIPPOLD J C, KISER S D.Welding Metallurgy and Weldability of Nickel-Base Alloys[M]. Chicago: John Wiley & Sons, 2009.
[27] CHAUVET E, TASSIN C, BLANDIN J J, et al.Producing Ni-Base Superalloys Single Crystal by Selective Electron Beam Melting[J]. Scripta Materialia, 2018, 152: 15-19.
[28] KARIMI P, SADEGHI E, ÅLGÅRDH J, et al. Columnar-to-Equiaxed Grain Transition in Powder Bed Fusion via Mimicking Casting Solidification and Promoting in Situ Recrystallization[J]. Additive Manufacturing, 2021, 46: 102086.
[29] LI Y, CHEN K, TAMURA N.Mechanism of Heat Affected Zone Cracking in Ni-Based Superalloy DZ125L Fabricated by Laser 3D Printing Technique[J]. Materials & Design, 2018, 150: 171-181.
[30] CLOOTS M, UGGOWITZER P J, WEGENER K.Investigations on the Microstructure and Crack Formation of IN738LC Samples Processed by Selective Laser Melting Using Gaussian and Doughnut Profiles[J]. Materials & Design, 2016, 89: 770-784.
[31] ENGELI R, ETTER T, HÖVEL S, et al. Processability of Different IN738LC Powder Batches by Selective Laser Melting[J]. Journal of Materials Processing Technology, 2016, 229: 484-491.
[32] RAMSPERGER M, MÚJICA RONCERY L, LOPEZ- GALILEA I, et al. Solution Heat Treatment of the Single Crystal Nickel-Base Superalloy CMSX-4 Fabricated by Selective Electron Beam Melting[J]. Advanced Engineering Materials, 2015, 17(10): 1486-1493.
[33] RAMSPERGER M, SINGER R F, KÖRNER C. Microstructure of the Nickel-Base Superalloy CMSX-4 Fabricated by Selective Electron Beam Melting[J]. Metallurgical and Materials Transactions A, 2016, 47(3): 1469-1480.
[34] MURR L E, MARTINEZ E, PAN X M, et al.Microstructures of Rene 142 Nickel-Based Superalloy Fabricated by Electron Beam Melting[J]. Acta Materialia, 2013, 61(11): 4289-4296.
[35] TANG Y T, PANWISAWAS C, GHOUSSOUB J N, et al.Alloys-by-Design: Application to New Superalloys for Additive Manufacturing[J]. Acta Materialia, 2021, 202: 417-436.
[36] GOEL S, SITTIHO A, CHARIT I, et al.Effect of Post-Treatments under Hot Isostatic Pressure on Microstructural Characteristics of EBM-Built Alloy 718[J]. Additive Manufacturing, 2019, 28: 727-737.
[37] SINGH S, ANDERSSON J, KADOI K.Microstructure Gradient Formation in Electron-Beam Melting Powder-Bed Fusion of a Gamma-Prime Ni-Based Superalloy[J]. Materials Characterization, 2023, 205: 113370.
[38] GHORPADE A, PRAKASH U, JOSHI S.Effect of Heat Treatments on Strengthening Mechanisms in Electron Beam Melted Superalloy Inconel 718[J]. Materials Science and Engineering: A, 2024, 895: 146232.
[39] CHAUVET E, KONTIS P, JÄGLE E A, et al. Hot Cracking Mechanism Affecting a Non-Weldable Ni- Based Superalloy Produced by Selective Electron Beam Melting[J]. Acta Materialia, 2018, 142: 82-94.
[40] RUTTERT B, RAMSPERGER M, MUJICA RONCERY L, et al.Impact of Hot Isostatic Pressing on Microstructures of CMSX-4 Ni-Base Superalloy Fabricated by Selective Electron Beam Melting[J]. Materials & Design, 2016, 110: 720-727.
[41] TAO S, GAO R, PENG H, et al.High-Reliability Repair of Single-Crystal Ni-Base Superalloy by Selective Electron Beam Melting[J]. Materials & Design, 2022, 224: 111421.
[42] AGHAJANI H, TOYSERKANI E.From Micro- to Macro-Cracks and Recrystallization in a Non-Weldable Ni-Based Superalloy Manufactured by Electron Beam Powder Bed Fusion[J]. Additive Manufacturing Letters, 2025, 15: 100323.
[43] PENG H, SHI Y, GONG S, et al.Microstructure, Mechanical Properties and Cracking Behaviour in a γ′- Precipitation Strengthened Nickel-Base Superalloy Fabricated by Electron Beam Melting[J]. Materials & Design, 2018, 159: 155-169.
[44] LUO M, RIELLI V V, FARABI E, et al.Grain Boundary Crystallography and Segregation in Ni-Based Superalloy INC738 Manufactured by Electron-Beam Powder Bed Fusion in As-Built and Annealed Conditions[J]. Materials Characterization, 2024, 217: 114421.
[45] DEHOFF R R, KIRKA M M, SAMES W J, et al.Site Specific Control of Crystallographic Grain Orientation through Electron Beam Additive Manufacturing[J]. Materials Science and Technology, 2015, 31(8): 931-938.
[46] KIRKA M M, UNOCIC K A, RAGHAVAN N, et al.Microstructure Development in Electron Beam-Melted Inconel 718 and Associated Tensile Properties[J]. JOM, 2016, 68(3): 1012-1020.
[47] CHAKRABORTY A, MUHAMMAD W, MASSE J P, et al.Role of Alloy Composition on Micro-Cracking Mechanisms in Additively Manufactured Ni-Based Superalloys[J]. Acta Materialia, 2023, 255: 119089.
[48] KOU S.A Criterion for Cracking during Solidification[J]. Acta Materialia, 2015, 88: 366-374.
[49] CHEN Y, ZHANG K, HUANG J, et al.Characterization of Heat Affected Zone Liquation Cracking in Laser Additive Manufacturing of Inconel 718[J]. Materials & Design, 2016, 90: 586-594.
[50] LUU D N, ZHOU W, NAI S M L. Mitigation of Liquation Cracking in Selective Laser Melted Inconel 718 through Optimization of Layer Thickness and Laser Energy Density[J]. Journal of Materials Processing Technology, 2022, 299: 117374.
[51] HAAS S, ANDERSSON J, FISK M, et al.Correlation of Precipitate Evolution with Vickers Hardness in Haynes282 Superalloy: In-Situ High-Energy SAXS/ WAXS Investigation[J]. Materials Science and Engineering: A, 2018, 711: 250-258.
[52] WANG Y F, WANG H Q, LI H, et al.The Porous Ni-Based Superalloy Manufactured by Customized Selective Electron Beam Melting Strategies: Pore Structure, Microstructures, Performance, and Computational Thermal Fluid Dynamics Simulation[J]. Journal of Manufacturing Processes, 2025, 142: 277-292.
[53] WEI L S, WANG Z H, WULIJI H, et al.Microcrack Mechanisms and Inhibition Strategies in Selective Laser Melting of Ni-Based Superalloys[J]. Journal of Alloys and Compounds, 2025, 1034: 181343.
[54] CUI H Y, TAN Y, NING L D, et al.Microstructure Control and Hot Cracking Behavior of the New Ni-Co Based Superalloy Prepared by Electron Beam Smelting Layered Solidification Technology[J]. Journal of Materials Science & Technology, 2024, 175: 55-71.
[55] CUI H Y, TAN Y, BAI R S, et al.Microsegregation of a New Ni-Co-Based Superalloy Prepared by Electron Beam Smelting Layered Solidification Technology and Its Homogenization Behavior[J]. Materials Characterization, 2022, 184: 111668.
[56] AGARWAL G, AMIRTHALINGAM M, MOON S C, et al.Experimental Evidence of Liquid Feeding during Solidification of a Steel[J]. Scripta Materialia, 2018, 146: 105-109.
[57] GOEL S, ZANINELLI E, GUNDGIRE T, et al.Microstructure Evolution and Mechanical Response-Based Shortening of Thermal Post-Treatment for Electron Beam Melting (EBM) Produced Alloy 718[J]. Materials Science and Engineering: A, 2021, 820: 141515.
[58] KONTIS P, CHAUVET E, PENG Z R, et al.Atomic-Scale Grain Boundary Engineering to Overcome Hot- Cracking in Additively-Manufactured Superalloys[J]. Acta Materialia, 2019, 177: 209-221.
[59] GRIFFITHS S, GHASEMI TABASI H, IVAS T, et al.Combining Alloy and Process Modification for Micro-Crack Mitigation in an Additively Manufactured Ni-Base Superalloy[J]. Additive Manufacturing, 2020, 36: 101443.
[60] GRIFFITHS S, GHASEMI-TABASI H, DE LUCA A, et al.Influence of Hf on the Heat Treatment Response of Additively Manufactured Ni-Base Superalloy CM247LC[J]. Materials Characterization, 2021, 171: 110815.
[61] CHENG X P, GUO Q Y, LIU C X, et al.Simultaneous Enhancement of Elevated Temperature Strength and Ductility in Additive-Manufactured Nickel-Based Superalloy via Doping Y2O3 Nanoparticles[J]. Journal of Materials Science & Technology, 2025, 210: 312-324.
[62] VIKRAM R J, KIRCHNER A, KLÖDEN B, et al. Optimized Heat Treatment for Electron Beam Powder Bed Fusion Processed IN718: Correlating Microstructure, Texture, and Mechanical Properties[J]. Advanced Engineering Materials, 2025, 27(9): 2401905.
[63] ZHAO X Y, DADBAKHSH S, RASHID A.Contouring Strategies to Improve the Tensile Properties and Quality of EBM Printed Inconel 625 Parts[J]. Journal of Manufacturing Processes, 2021, 62: 418-429.

Funding

National Key R&D Program of China (2023YFB4605000)
PDF(1805 KB)

Accesses

Citation

Detail

Sections
Recommended

/