Hot Deformation Behavior and Microstructure Evolution of As-cast Ni-Cr-Co-based Superalloy

SHA Lei, ZHONG Kangdi, WANG Bingbing, MA Pingdong

Journal of Netshape Forming Engineering ›› 2026, Vol. 18 ›› Issue (4) : 155-166.

PDF(6287 KB)
PDF(6287 KB)
Journal of Netshape Forming Engineering ›› 2026, Vol. 18 ›› Issue (4) : 155-166. DOI: 10.3969/j.issn.1674-6457.2026.04.016
Superalloy Forming

Hot Deformation Behavior and Microstructure Evolution of As-cast Ni-Cr-Co-based Superalloy

  • SHA Lei1,2, ZHONG Kangdi1,2,*, WANG Bingbing1,2, MA Pingdong3
Author information +
History +

Abstract

The work aims to investigate the hot deformation behavior and microstructure evolution of an as-cast precipitation-strengthened Ni-Cr-Co-based superalloy under varying thermomechanical parameters, elucidate dynamic recrystallization (DRX) nucleation mechanisms, and provide theoretical support for optimizing the cogging process and microstructure control of as-cast superalloy. Hot compression tests were performed on a Gleeble-3800 thermomechanical simulator within temperature ranges of 1 030-1 150 ℃, strain rates of 0.01-10 s-1, and true strains of 0.16-0.92. The flow stress characteristics under varying deformation parameters were analyzed. Electron backscatter diffraction (EBSD), backscattered electron (BSE) imaging, and transmission electron microscopy (TEM) were utilized to investigate the effects of different deformation temperature and strain levels on the microstructure morphology and evolution with a focus on DRX nucleation mechanisms. The results showed that the flow stress of as-cast Ni-Cr-Co based superalloy increased with the decrease of temperature or the increase of strain rate, and the stress-strain curves exhibited typical DRX characteristics. DRX grain size and volume fraction increased with the increase of deformation temperature. At lower temperature (1 030 ℃), DRX grains were distributed in agglomerated clusters, and the degree of recrystallization progressed slowly with the increase of strain. At higher temperature (1 150 ℃), the coarsened DRX grains were distributed in a "necklace" shape along the grain boundary and formed a homogeneous structure under high strain. At 1 060 ℃, discontinuous dynamic recrystallization ( DDRX ) and continuous dynamic recrystallization (CDRX) coexisted, with particle-stimulated nucleation (PSN) induced by γ′ phase pinning dislocations and grain boundary bulging dominating as primary nucleation mechanisms, while CDRX served as an auxiliary mechanism. At 1 150 ℃, DDRX through grain boundary bulging became the predominant mechanism, and the overall contribution of CDRX decreased. By studying the hot deformation flow behavior, microstructure evolution and DRX mechanism of an as-cast Ni-Cr-Co-based superalloy with different deformation parameters, the influence of deformation parameters and γ' precipitates on the microstructure and nucleation mechanism of hot deformation is obtained, which can be used to optimize the process parameters and microstructure control of Ni-Cr-Co-based superalloy ingots.

Key words

as-cast Ni-Cr-Co-based superalloy / hot deformation / DRX / microstructure / DRX mechanism

Cite this article

Download Citations
SHA Lei, ZHONG Kangdi, WANG Bingbing, MA Pingdong. Hot Deformation Behavior and Microstructure Evolution of As-cast Ni-Cr-Co-based Superalloy[J]. Journal of Netshape Forming Engineering. 2026, 18(4): 155-166 https://doi.org/10.3969/j.issn.1674-6457.2026.04.016

References

[1] 田曾, 金万军, 王倩, 等. 冷拔态GH4738合金热变形本构方程及热加工图[J]. 精密成形工程, 2024, 16(5): 193-200.
TIAN Z, JIN W J, WANG Q, et al.Constitutive Equation for Hot Deformation and Hot Processing Map of Cold-Drawn GH4738 Alloy[J]. Journal of Netshape Forming Engineering, 2024, 16(5): 193-200.
[2] 牛庆伟, 郝敬宾, 纪皓文, 等. 超声辅助激光熔覆IN 625高温合金涂层组织及性能研究[J]. 精密成形工程, 2024, 16(2): 137-148.
NIU Q W, HAO J B, JI H W, et al.Microstructure and Properties of IN 625 High-Temperature Alloy Coating by Ultrasonic Assisted Laser Cladding[J]. Journal of Netshape Forming Engineering, 2024, 16(2): 137-148.
[3] YANG J L, CUI J Y, CHENG J Y, et al.Hot Deformation Behavior and Microstructure Evolution of a Novel Nickel-Based Powder Metallurgy Superalloy[J]. Journal of Materials Research and Technology, 2023, 27: 7347-7363.
[4] 丁雨田, 闫康, 马元俊, 等. 一种新型Ni-Cr-Co基变形高温合金的均匀化工艺[J]. 稀有金属, 2023, 47(10): 1342-1351.
DING Y T, YAN K, MA Y J, et al.Homogenization of a New-Type Ni-Cr-Co Based Wrought Superalloy[J]. Chinese Journal of Rare Metals, 2023, 47(10): 1342-1351.
[5] 周标, 符锐, 姚志浩, 等. 重型燃气轮机用Ni-Cr-Co基高温合金组织稳定性研究[J]. 动力工程学报, 2022, 42(6): 582-588.
ZHOU B, FU R, YAO Z H, et al.Microstructure Stability of Ni-Cr-Co Based Superalloy for Heavy-Duty Gas Turbine[J]. Journal of Chinese Society of Power Engineering, 2022, 42(6): 582-588.
[6] 李慧中, 杨雷, 王岩, 等. 热挤压态Ni-Co-Cr基粉末高温合金热加工行为[J]. 材料工程, 2020, 48(9): 115-123.
LI H Z, YANG L, WANG Y, et al.Hot Working Behavior of Hot-Extruded Ni-Co-Cr-Based Powder Metallurgy Superalloy[J]. Journal of Materials Engineering, 2020, 48(9): 115-123.
[7] LI Y S, DONG Y W, JIANG Z H, et al.Hot Deformation Characteristics of GH4975 Nickel-Based Superalloy in the Coexistence Region of γ and γ′ Phases[J]. JOM, 2024, 76(9): 5133-5148.
[8] XIE B C, ZHANG B Y, YU H, et al.Microstructure Evolution and Underlying Mechanisms during the Hot Deformation of 718Plus Superalloy[J]. Materials Science and Engineering: A, 2020, 784: 139334.
[9] 王兴茂, 丁雨田, 高钰璧, 等. 一种新型Ni-Cr-Co基合金的热变形行为及其组织演变[J]. 稀有金属材料与工程, 2022, 51(1): 249-259.
WANG X M, DING Y T, GAO Y B, et al.Hot Deformation Behavior and Microstructure Evolution of New-Type Ni-Cr-Co Based Alloy[J]. Rare Metal Materials and Engineering, 2022, 51(1): 249-259.
[10] LI H Z, LIU X G, ZHANG W W, et al.Microstructure Evolution and Dynamic Recrystallization Mechanism during Thermal Deformation of GH4698 Superalloy[J]. Journal of Materials Science, 2022, 57(4): 2969-2987.
[11] HE G A, LIU F, HUANG L, et al.Microstructure Evolutions and Nucleation Mechanisms of Dynamic Recrystallization of a Powder Metallurgy Ni-Based Superalloy during Hot Compression[J]. Materials Science and Engineering: A, 2016, 677: 496-504.
[12] XIE B C, YU H, SHENG T, et al.DDRX and CDRX of an As-Cast Nickel-Based Superalloy during Hot Compression at γ′ Sub-/Super-Solvus Temperatures[J]. Journal of Alloys and Compounds, 2019, 803: 16-29.
[13] JIA D, SUN W R, XU D S, et al.Dynamic Recrystallization Behavior of GH4169G Alloy during Hot Compressive Deformation[J]. Journal of Materials Science & Technology, 2019, 35(9): 1851-1859.
[14] 凌文丹, 王海瑞, 赵平堂, 等. GH4141高温合金热压缩变形特性研究[J]. 特种铸造及有色合金, 2023, 43(7): 902-907.
LING W D, WANG H R, ZHAO P T, et al.Deformation Characteristics of GH4141 Superalloy under Hot Compression[J]. Special Casting & Nonferrous Alloys, 2023, 43(7): 902-907.
[15] CHEN X M, LIN Y C, WEN D X, et al.Dynamic Recrystallization Behavior of a Typical Nickel-Based Superalloy during Hot Deformation[J]. Materials & Design, 2014, 57: 568-577.
[16] TAN Y B, MA Y H, ZHAO F.Hot Deformation Behavior and Constitutive Modeling of Fine Grained Inconel 718 Superalloy[J]. Journal of Alloys and Compounds, 2018, 741: 85-96.
[17] SOMMITSCH C, MITTER W.On Modelling of Dynamic Recrystallisation of Fcc Materials with Low Stacking Fault Energy[J]. Acta Materialia, 2006, 54(2): 357-375.
[18] YANG J, LUO J, LI X Y, et al.Evolution Mechanisms of Recrystallized Grains and Twins during Isothermal Compression and Subsequent Solution Treatment of GH4586 Superalloy[J]. Journal of Alloys and Compounds, 2021, 850: 156732.
[19] BETANDA Y A, HELBERT A, BRISSET F, et al.Measurement of Stored Energy in Fe-48%Ni Alloys Strongly Cold-Rolled Using Three Approaches: Neutron Diffraction, Dillamore and KAM Approaches[J]. Materials Science and Engineering: A, 2014, 614: 193-198.
[20] LIU P, ZHANG R, YUAN Y, et al.Microstructural Evolution of a Ni-Co Based Superalloy during Hot Compression at γ′ Sub-/Super-Solvus Temperatures[J]. Journal of Materials Science & Technology, 2021, 77: 66-81.
[21] YU H, WANG Z T, NING Y Q, et al.DRX Mechanisms of a Ni-Co-W Type Superalloy with Typical Columnar Grains during Hot Compression[J]. Journal of Alloys and Compounds, 2023, 959: 170533.
[22] XIE B C, ZHANG B Y, NING Y Q, et al.Mechanisms of DRX Nucleation with Grain Boundary Bulging and Subgrain Rotation during the Hot Working of Nickel-Based Superalloys with Columnar Grains[J]. Journal of Alloys and Compounds, 2019, 786: 636-647.
[23] TIAMIYU A A, PANG E L, CHEN X, et al.Nanotwinning-Assisted Dynamic Recrystallization at High Strains and Strain Rates[J]. Nature Materials, 2022, 21(7): 786-794.
[24] ZHANG B Y, WANG Z T, YU H, et al.Microstructural Origin and Control Mechanism of the Mixed Grain Structure in Ni-based Superalloys[J]. Journal of Alloys and Compounds, 2022, 900: 163515.
[25] WU H, LIU M X, WANG Y, et al.Experimental Study and Numerical Simulation of Dynamic Recrystallization for a FGH96 Superalloy during Isothermal Compression[J]. Journal of Materials Research and Technology, 2020, 9(3): 5090-5104.

Funding

Natural Science Foundation of Xinjiang Uygur Autonomous Region Youth Project (2025D01C342, 2024D01C210, 2022D01C738)
PDF(6287 KB)

Accesses

Citation

Detail

Sections
Recommended

/