Microstructure and Properties of Magnesium Alloy Bar during Radial Forging-extrusion Forming Process

ZOU Jingfeng, GUO Xingchen, SUN Dong, ZHU Yanchun, LI Yitao, HE Zhiqiang, GAO Feiyang

Journal of Netshape Forming Engineering ›› 2025, Vol. 17 ›› Issue (11) : 190-200.

PDF(25180 KB)
PDF(25180 KB)
Journal of Netshape Forming Engineering ›› 2025, Vol. 17 ›› Issue (11) : 190-200. DOI: 10.3969/j.issn.1674-6457.2025.11.018
Light Alloy Forming

Microstructure and Properties of Magnesium Alloy Bar during Radial Forging-extrusion Forming Process

  • ZOU Jingfeng1,2,*, GUO Xingchen1,3, SUN Dong1, ZHU Yanchun1,3, LI Yitao1,2, HE Zhiqiang1,3, GAO Feiyang1,3
Author information +
History +

Abstract

The work aims to realize the simultaneous improvement in strength and ductility for ZK60 magnesium alloy bars through an integrated radial forging and extrusion process. Finite element simulations via Deform software were employed to analyze the macroscopic stress distribution and strain gradient evolution during both radial forging and subsequent hot extrusion. The radial forging and hot extrusion experiment with large-scale billets was conducted to investigate the microstructural evolution and mechanical properties of bar stocks after composite process treatment to reveal the effect mechanism of macroscopic stress on microstructure and properties. The radial forging effectively fragmented the coarse as-cast microstructure, producing remarkable grain refinement along the axial direction while generating a distinct radial grain size gradient from surface to center. Numerical simulations correlated this graded microstructure with the corresponding strain gradient, additionally revealing the formation of a strong basal texture in the subsurface region. Following high-ratio extrusion (25∶1), the grains were further refined and the texture intensity was weakened, resulting in a typical fibrous texture. Compared with as-cast bars, the bars processed by radial forging-extrusion exhibited substantially enhanced mechanical properties, with tensile strength increasing from 208 MPa to 400 MPa, yield strength from 84 MPa to 263 MPa, and elongation from 8.5% to 23.5%. The radial forging-extrusion process can effectively improve the microstructural homogeneity of ZK60 magnesium alloy bars, achieving a synergistic enhancement of strength and plasticity, which is attributed to the combined effects of grain refinement, second-phase strengthening, and dislocation strengthening.

Key words

magnesium alloy / radial forging / hot extrusion / microstructure / texture

Cite this article

Download Citations
ZOU Jingfeng, GUO Xingchen, SUN Dong, ZHU Yanchun, LI Yitao, HE Zhiqiang, GAO Feiyang. Microstructure and Properties of Magnesium Alloy Bar during Radial Forging-extrusion Forming Process[J]. Journal of Netshape Forming Engineering. 2025, 17(11): 190-200 https://doi.org/10.3969/j.issn.1674-6457.2025.11.018

References

[1] DONG X X, FENG L Y, WANG S H, et al.A New Die-Cast Magnesium Alloy for Applications at Higher Elevated Temperatures of 200-300℃[J]. Journal of Magnesium and Alloys, 2021, 9(1): 90-101.
[2] ZOU J F, MA L F, ZHU Y C, et al.Gradient Microstructure and Superior Strength-Ductility Synergy of AZ61 Magnesium Alloy Bars Processed by Radial Forging with Different Deformation Temperatures[J]. Journal of Materials Science & Technology, 2024, 170: 65-77.
[3] 胡雕, 马旻, 陈曦, 等. 应变速率对衬板轧制AZ31镁合金组织和力学性能的影响[J]. 精密成形工程, 2024, 16(11): 65-74.
HU D, MA M, CHEN X, et al.Effect of Strain Rate on Microstructure and Mechanical Properties of Hard Plate Rolled AZ31 Magnesium Alloy[J]. Journal of Netshape Forming Engineering, 2024, 16(11): 65-74.
[4] HIRSCH J, AL-SAMMAN T.Superior Light Metals by Texture Engineering: Optimized Aluminum and Magnesium Alloys for Automotive Applications[J]. Acta Materialia, 2013, 61(3): 818-843.
[5] CHEN B, LIN D L, JIN L, et al.Equal-Channel Angular Pressing of Magnesium Alloy AZ91 and Its Effects on Microstructure and Mechanical Properties[J]. Materials Science and Engineering: A, 2008, 483: 113-116.
[6] PÉREZ-PRADO M T, VALLE J A, RUANO O A. Achieving High Strength in Commercial Mg Cast Alloys through Large Strain Rolling[J]. Materials Letters, 2005, 59(26): 3299-3303.
[7] LIN J B, WANG Q D, CHEN Y J, et al.Microstructure and Texture Characteristics of ZK60 Mg Alloy Processed by Cyclic Extrusion and Compression[J]. Transactions of Nonferrous Metals Society of China, 2010, 20(11): 2081-2085.
[8] VALIEV R Z, ISLAMGALIEV R K, ALEXANDROV I V.Bulk Nanostructured Materials from Severe Plastic Deformation[J]. Progress in Materials Science, 2000, 45(2): 103-189.
[9] XU C, ZHENG M Y, XU S W, et al.Microstructure and Mechanical Properties of Mg-Gd-Y-Zn-Zr Alloy Sheets Processed by Combined Processes of Extrusion, Hot Rolling and Ageing[J]. Materials Science and Engineering: A, 2013, 559: 844-851.
[10] DU Z M, WANG D Y, ZHANG H J.Influence of Hot Extrusion Process on Microstructure and Mechanical Properties of Mg-Zn-Y-Zr Magnesium Alloy[J]. Rare Metal Materials and Engineering, 2018, 47(6): 1655-1661.
[11] MURAI T, MATSUOKA S I, MIYAMOTO S, et al.Effects of Extrusion Conditions on Microstructure and Mechanical Properties of AZ31B Magnesium Alloy Extrusions[J]. Journal of Materials Processing Technology, 2003, 141(2): 207-212.
[12] KLEINER S, UGGOWITZER P J.Mechanical Anisotropy of Extruded Mg-6% Al-1% Zn Alloy[J]. Materials Science and Engineering: A, 2004, 379(1/2): 258-263.
[13] ZHAO T S, HU Y B, ZHANG C, et al.Influence of Extrusion Conditions on Microstructure and Mechanical Properties of Mg-2Gd-0.3Zr Magnesium Alloy[J]. Journal of Magnesium and Alloys, 2022, 10(2): 387-399.
[14] PENG P, SHE J, TANG A T, et al.Novel Continuous Forging Extrusion in a One-Step Extrusion Process for Bulk Ultrafine Magnesium Alloy[J]. Materials Science and Engineering: A, 2019, 764: 138144.
[15] 张晋华, 聂凯波, 邓坤坤, 等. 锻造+挤压复合变形对SiCp/Mg-Zn-Y-Ca复合材料组织与性能的影响[J]. 材料热处理学报, 2022, 43(2): 1-9.
ZHANG J H, NIE K B, DENG K K, et al.Effect of Forging and Extrusion Combined Deformation on Microstructure and Properties of SiCp/Mg-Zn-Y-Ca Composites[J]. Transactions of Materials and Heat Treatment, 2022, 43(2): 1-9.
[16] ZOU J F, MA L F, JIA W T, et al.Microstructural and Mechanical Response of ZK60 Magnesium Alloy Subjected to Radial Forging[J]. Journal of Materials Science & Technology, 2021, 83: 228-238.
[17] MA X, DE ROOIJ M B, SCHIPPER D J. Friction Conditions in the Bearing Area of an Aluminium Extrusion Process[J]. Wear, 2012, 278: 1-8.
[18] YU J Q, ZHAO G Q, CHEN L.Analysis of Longitudinal Weld Seam Defects and Investigation of Solid-State Bonding Criteria in Porthole Die Extrusion Process of Aluminum Alloy Profiles[J]. Journal of Materials Processing Technology, 2016, 237: 31-47.
[19] WU Y J, DONG X H, YU Q.An Upper Bound Solution of Axial Metal Flow in Cold Radial Forging Process of Rods[J]. International Journal of Mechanical Sciences, 2014, 85: 120-129.
[20] YU H, PARK S H, YOU B S.Die Angle Dependency of Microstructural Inhomogeneity in an Indirect-Extruded AZ31 Magnesium Alloy[J]. Journal of Materials Processing Technology, 2015, 224: 181-188.
[21] 董节功, 周旭东, 朱锦洪, 等. 径向锻造三维成形锻透性的数值模拟[J]. 机械工程材料, 2007, 31(3): 76-78.
DONG J G, ZHOU X D, ZHU J H, et al.FEM Simulation of Forging Penetration Efficiency of Radial Forging in 3D[J]. Materials for Mechanical Engineering, 2007, 31(3): 76-78.
[22] MAYAMA T, NODA M, CHIBA R, et al.Crystal Plasticity Analysis of Texture Development in Magnesium Alloy during Extrusion[J]. International Journal of Plasticity, 2011, 27(12): 1916-1935.
[23] MABUCHI M, KUBOTA K, HIGASHI K.New Recycling Process by Extrusion for Machined Chips of AZ91 Magnesium and Mechanical Properties of Extruded Bars[J]. Materials Transactions, JIM, 1995, 36(10): 1249-1254.
[24] WU H Y, YANG J C, ZHU F J, et al.Hot Deformation Characteristics of As-Cast and Homogenized AZ61 Mg Alloys under Compression[J]. Materials Science and Engineering: A, 2012, 550: 273-278.
[25] YANG Y, YANG X Y, XIAO Z Y, et al.Annealing Behavior of a Cast Mg-Gd-Y-Zr Alloy with Necklace Fine Grains Developed under Hot Deformation[J]. Materials Science and Engineering: A, 2017, 688: 280-288.
[26] GALIYEV A, KAIBYSHEV R, GOTTSTEIN G.Correlation of Plastic Deformation and Dynamic Recrystallization in Magnesium Alloy ZK60[J]. Acta Materialia, 2001, 49(7): 1199-1207.
[27] HUANG K, LOGÉ R E.A Review of Dynamic Recrystallization Phenomena in Metallic Materials[J]. Materials & Design, 2016, 111: 548-574.
[28] WANG H Y, YU Z P, ZHANG L, et al.Achieving High Strength and High Ductility in Magnesium Alloy Using Hard-Plate Rolling (HPR) Process[J]. Scientific Reports, 2015, 5: 17100.
[29] XU Y Y, LIANG Y L, PENG G G.Effect of a Compound Modification Process on the Microstructure and Mechanical Properties of ZK60 Magnesium Alloys[J]. Materials Science and Engineering: A, 2020, 778: 139117.
[30] KARPARVARFARD S M H, SHAHA S K, BEHRAVESH S B, et al. Microstructure, Texture and Mechanical Behavior Characterization of Hot Forged Cast ZK60 Magnesium Alloy[J]. Journal of Materials Science & Technology, 2017, 33(9): 907-918.
[31] HADORN J P, SASAKI T T, NAKATA T, et al.Solute Clustering and Grain Boundary Segregation in Extruded Dilute Mg-Gd Alloys[J]. Scripta Materialia, 2014, 93: 28-31.
[32] JIANG M G, YAN H, CHEN R S.Twinning, Recrystallization and Texture Development during Multi-Directional Impact Forging in an AZ61 Mg Alloy[J]. Journal of Alloys and Compounds, 2015, 650: 399-409.
[33] GODET S, JIANG L, LUO A A, et al.Use of Schmid Factors to Select Extension Twin Variants in Extruded Magnesium Alloy Tubes[J]. Scripta Materialia, 2006, 55(11): 1055-1058.
[34] PETCH N J.The Cleavage Strength of Polycrystals[J]. Journal of the Iron and Steel Institute, 1953, 174(19): 25-28
[35] YANG Z, LI J P, GUO Y C, et al.Precipitation Process and Effect on Mechanical Properties of Mg-9Gd-3Y- 0.6Zn-0.5Zr Alloy[J]. Materials Science and Engineering: A, 2007, 454: 274-280.
[36] ZHOU J X, YANG H, XIE W L, et al.A Novel Strategy Synergistically Enhances the Strength and Ductility of Mg-Gd-Zr Alloys by Tailoring a Heterogeneous Structure[J]. Journal of Alloys and Compounds, 2025, 1022: 179782.
[37] 王鸿, 颜银标, 沈骏. 多方向锻造对ZK60镁合金组织和力学性能的影响[J]. 热加工工艺, 2014, 43(21): 47-49.
WANG H, YAN Y B, SHEN J.Effect of Multi-Directional Forging on Microstructure and Mechanical Properties of Magnesium Alloy ZK60[J]. Hot Working Technology, 2014, 43(21): 47-49.
[38] 包娜娜, 许道奎, 刘春忠. 固溶后的晶粒结构对ZK60镁合金挤压型材力学性能的影响[J]. 金属热处理, 2018, 43(9): 64-69.
BAO N N, XU D K, LIU C Z.Influence of Grain Structure after Solid Solution on Mechanical Properties of ZK60 Alloy Extruded Profiles[J]. Heat Treatment of Metals, 2018, 43(9): 64-69.
[39] 薄东明, 卢遥, 孙静娜, 等. 轧制方式对ZK60镁合金组织与性能的影响[J]. 精密成形工程, 2023, 15(12): 1-11.
BO D M, LU Y, SUN J N, et al.Effect of Rolling Methods on Microstructure and Properties of ZK60 Magnesium Alloy[J]. Journal of Netshape Forming Engineering, 2023, 15(12): 1-11.

Funding

National Natural Science Foundation of China (52205400, 52375363); Fundamental Research Program of Shanxi Province (202203021212321); The Authors Gratefully Acknowledge the National Key Research and Development Program (2024YFB3714303); Shanxi Provincial Science & Technology Achievements Transformation Guidance Program (202404021301041)
PDF(25180 KB)

Accesses

Citation

Detail

Sections
Recommended

/