Hot Deformation Behavior and Superplastic Extrusion Forming of Magnesium-lithium Alloys

LYU Yunxiang, DONG Ying, FU Wenliang, GAO Shiqing, XIA Xiangsheng, LU Zhen

Journal of Netshape Forming Engineering ›› 2025, Vol. 17 ›› Issue (8) : 52-59.

PDF(7339 KB)
PDF(7339 KB)
Journal of Netshape Forming Engineering ›› 2025, Vol. 17 ›› Issue (8) : 52-59. DOI: 10.3969/j.issn.1674-6457.2025.08.006
Light Alloy Forming

Hot Deformation Behavior and Superplastic Extrusion Forming of Magnesium-lithium Alloys

  • LYU Yunxiang1, DONG Ying2,*, FU Wenliang3, GAO Shiqing4, XIA Xiangsheng4, LU Zhen1,*
Author information +
History +

Abstract

The work aims to realize the high-performance forming of magnesium-lithium alloy components through plastic forming processes. The hot deformation behavior of as-cast LAZ931 magnesium-lithium alloys at various temperatures and strain rates was investigated via hot compression tests. Magnesium-lithium alloy forgings were fabricated by multi-directional forging technology and formed through isothermal superplastic extrusion. The as-cast magnesium-lithium alloy demonstrated excellent hot deformation performance, but it was prone to instability at low temperatures and high strain rates, and the zone of hot processing instability gradually expanded with the increase in deformation. Multi-directional forging could significantly refine the two-phase microstructure through dynamic recrystallization, allowing the alloy to acquire good superplastic deformation ability. The elongation and flow resistance of the forged alloy at 300 ℃ and a strain rate of 5×10-4 s-1 reached over 200% and approximately 8 MPa, respectively. The forming of cylinder components was accomplished through superplastic extrusion forming. After forming, the mechanical room temperature yield strength, tensile strength, and elongation reached approximately 163 MPa, 197 MPa, and 22%, respectively, which increased by 20.7%, 19.4%, and 83%, respectively, compared to those of the as-cast alloy. The hot deformation behavior of magnesium-lithium alloys is investigated through hot compression deformation. Its flow stress decreases with the rise in temperature and increases with the increase in strain rate, presenting a positive strain rate sensitivity. Cylinder structures of magnesium-lithium alloys with favorable comprehensive properties can be prepared by superplastic isothermal extrusion.

Key words

magnesium-lithium alloy / superplastic forming / hot processing map / microstructure morphology

Cite this article

Download Citations
LYU Yunxiang, DONG Ying, FU Wenliang, GAO Shiqing, XIA Xiangsheng, LU Zhen. Hot Deformation Behavior and Superplastic Extrusion Forming of Magnesium-lithium Alloys[J]. Journal of Netshape Forming Engineering. 2025, 17(8): 52-59 https://doi.org/10.3969/j.issn.1674-6457.2025.08.006

References

[1] LI J F, ZHENG Z Q, LI S C, et al.Preparation and Galvanic Anodizing of a Mg-Li Alloy[J]. Materials Science and Engineering: A, 2006, 433(1/2): 233-240.
[2] MORDIKE B L, EBERT T.Magnesium Properties- Applications-Potential[J]. Materials Science and Engineering: A, 2001, 302(1): 37-45.
[3] 冯凯, 李丹明, 何成旦, 等. 航天用超轻镁锂合金研究进展[J]. 特种铸造及有色合金, 2017, 37(2): 140-144.
FENG K, LI D M, HE C D, et al.Progress in Superlight Mg-Li Alloys for Aerospace Industry[J]. Special Casting & Nonferrous Alloys, 2017, 37(2): 140-144.
[4] 田光元, 王俊升. 高强高模铸造镁锂合金的制备及性能综述[J]. 航空制造技术, 2025, 68(8): 94-104.
TIAN G Y, WANG J S.A Review of Preparation and Performance of High-Strength and High-Modulus Casting Mg-Li Alloy[J]. Aeronautical Manufacturing Technology, 2025, 68(8): 94-104.
[5] SONG W J, LIU J, HE S, et al. Microstructure and Mechanical Properties of As-Cast Ultralight and High Strength Mg-10Li-3Al-3Zn-xY Alloy with Multi-Prec- ipitates[J]. Materials Characterization, 2022, 189: 1119 72.
[6] 吴利斌, 孟祥瑞, 崔崇亮, 等. 超轻变形Mg-Li-Al-Zn合金的显微组织和性能[J]. 铸造技术, 2009, 30(10): 1256-1259.
WU L B, MENG X R, CUI C L, et al.Microstructures and Properties of Superlight Mg-Li-Al-Zn Wrought Alloys[J]. Foundry Technology, 2009, 30(10): 1256-1259.
[7] 孟宝, 潘丰, 万敏. 电场辅助镁锂合金超塑变形行为及其在微型热管成形中的应用[J]. 塑性工程学报, 2023, 30(6): 142-150.
MENG B, PAN F, WAN M.Electric Field Assisted Superplastic Deformation Behavior of Mg-Li Alloy and Its Application in Micro Heat Pipe Forming[J]. Journal of Plasticity Engineering, 2023, 30(6): 142-150.
[8] 冯效琰, 李瑞红, 张晓梅, 等. 两道次挤压Mg-5Li-1Al镁锂合金的力学性能及成形性[J]. 内蒙古科技大学学报, 2020, 39(2): 47-51.
FENG X Y, LI R H, ZHANG X M, et al.Mechanical Properties and Formability of Two-Pass Extruded Mg-5Li-1Al Alloy Sheet[J]. Journal of Inner Mongolia University of Science and Technology, 2020, 39(2): 47-51.
[9] 曾朝伟, 袁婷, 彭威, 等. 塑性成形方法对镁合金耐蚀性的影响及展望[J]. 精密成形工程, 2023, 15(7): 104-119.
ZENG C W, YUAN T, PENG W, et al.Effect of Plastic Forming Method on Corrosion Resistance of Magnesium Alloy and Its Prospects[J]. Journal of Netshape Forming Engineering, 2023, 15(7): 104-119.
[10] XU T C, PENG X D, QIN J, et al.Dynamic Recrystallization Behavior of Mg-Li-Al-Nd Duplex Alloy during Hot Compression[J]. Journal of Alloys and Compounds, 2015, 639: 79-88.
[11] LIU G, XIE W, WEI G B, et al.Dynamic Recrystallization Behavior and Corrosion Resistance of a Dual-Phase Mg-Li Alloy[J]. Materials, 2018, 11(3): 408.
[12] MUGA C, GUO H, ZOU Y, et al.Effects of Holmium and Hot-Rolling on Microstructure and Mechanical Properties of Mg-Li Based Alloys[J]. Journal of Rare Earths, 2016, 34(12): 1269-1276.
[13] HOU L G, WANG T Z, WU R Z, et al.Microstructure and Mechanical Properties of Mg-5Li-1Al Sheets Prepared by Accumulative Roll Bonding[J]. Journal of Materials Science & Technology, 2018, 34(2): 317-323.
[14] 贾玉鑫, 黄金亮, 冯剑. 固溶时效处理对轧制态Mg-12Li-2Al-1Zn合金组织与性能的影响[J]. 金属热处理, 2014, 39(1): 7-10.
JIA Y X, HUANG J L, FENG J.Effects of Solid Solution and Aging Treatment on Microstructure and Mechanical Properties of Mg-12Li-2Al-1Zn Alloy As-Rolled[J]. Heat Treatment of Metals, 2014, 39(1): 7-10.
[15] ZHANG Y, ZHANG J, WU G H, et al.Microstructure and Tensile Properties of As-Extruded Mg-Li-Zn-Gd Alloys Reinforced with Icosahedral Quasicrystal Phase[J]. Materials & Design (1980-2015), 2015, 66: 162-168.
[16] 马骏, 樊晓泽, 王瑞, 等. 不同挤压温度对LA103Z镁锂合金组织与性能的影响[J]. 铸造设备与工艺, 2022(3): 48-50.
MA J, FAN X Z, WANG R, et al.Different Extrusion Temperature on Microstructure and Properties of LA103Z Magnesium Lithium Alloy[J]. Foundry Equipment & Technology, 2022(3): 48-50.
[17] 火照燕, 马勤, 完彦少君. 等通道转角挤压对LA141镁锂合金显微组织及力学性能的影响[J]. 热加工工艺, 2019, 48(7): 32-35.
HUO Z Y, MA Q, WANYAN S J.Effect of ECAP on Microstructure and Mechanical Properties of LA141 Mg-Li Alloy[J]. Hot Working Technology, 2019, 48(7): 32-35.
[18] KARAMI M, MAHMUDI R.Work Hardening Behavior of the Extruded and Equal-Channel Angularly Pressed Mg-Li-Zn Alloys under Tensile and Shear Deformation Modes[J]. Materials Science and Engineering: A, 2014, 607: 512-520.
[19] LENTZ M, KLAUS M, BEYERLEIN I J, et al.In Situ X-Ray Diffraction and Crystal Plasticity Modeling of the Deformation Behavior of Extruded Mg-Li-(Al) Alloys: An Uncommon Tension-Compression Asymmetry[J]. Acta Materialia, 2015, 86: 254-268.
[20] ZHOU Y C, CHEN Z Y, JI J, et al.Optimization of Hot Deformation Parameters and Constitutive Analysis for As-Cast Mg-5Li-3Zn-0.3Y Alloy Using Processing Ma- ps[J]. Journal of Materials Engineering and Performance, 2018, 27(9): 4606-4615.
[21] KARAMI M, MAHMUDI R.Hot Shear Deformation Constitutive Analysis of an Extruded Mg-6Li-1Zn Alloy[J]. Materials Letters, 2012, 81: 235-238.
[22] 舒帆, 车朝杰, 程丽任. 铸态Mg-2Sc-2Y-0.5Zr合金热压缩行为及热加工图[J]. 精密成形工程, 2023, 15(3): 1-8.
SHU F, CHE C J, CHENG L R.Hot Compression Behavior and Processing Map of As-Cast Mg-2Sc-2Y-0.5 Zr Alloy[J]. Journal of Netshape Forming Engineering, 2023, 15(3): 1-8.
[23] SHALBAFI M, ROUMINA R, MAHMUDI R.Hot Deformation of the Extruded Mg-10Li-1Zn Alloy: Constitutive Analysis and Processing Maps[J]. Journal of Alloys and Compounds, 2017, 696: 1269-1277.
[24] WAN Z P, HU L X, SUN Y, et al.Hot Deformation Behavior and Processing Workability of a Ni-Based Alloy[J]. Journal of Alloys and Compounds, 2018, 769: 367-375.
[25] HE D G, LIN Y C, CHEN M S, et al.Effect of Pre-Treatment on Hot Deformation Behavior and Processing Map of an Aged Nickel-Based Superalloy[J]. Journal of Alloys and Compounds, 2015, 649: 1075-1084.
[26] PU E X, ZHENG W J, SONG Z G, et al.Hot Deformation Characterization of Nickel-Based Superalloy UNS10276 through Processing Map and Microstructural Studies[J]. Journal of Alloys and Compounds, 2017, 694: 617-631.
[27] LI D H, YANG Y, XU T, et al.Observation of the Microstructure in the Adiabatic Shear Band of 7075 Aluminum Alloy[J]. Materials Science and Engineering: A, 2010, 527(15): 3529-3535.
[28] JIANG L, JONAS J J, MISHRA R K, et al.Twinning and Texture Development in Two Mg Alloys Subjected to Loading along Three Different Strain Paths[J]. Acta Materialia, 2007, 55(11): 3899-3910.
PDF(7339 KB)

Accesses

Citation

Detail

Sections
Recommended

/