新型Ni-Cr-Fe基高温合金热变形行为研究

杜方鑫, 赵聪, 刘晋平, 刘劲松

精密成形工程 ›› 2025, Vol. 17 ›› Issue (9) : 176-184.

PDF(6913 KB)
PDF(6913 KB)
精密成形工程 ›› 2025, Vol. 17 ›› Issue (9) : 176-184. DOI: 10.3969/j.issn.1674-6457.2025.09.017
高温合金成形

新型Ni-Cr-Fe基高温合金热变形行为研究

  • 杜方鑫1,*, 赵聪1, 刘晋平2, 刘劲松1
作者信息 +

Hot Deformation Behavior of a Novel Ni-Cr-Fe Based Superalloy

  • DU Fangxin1,*, ZHAO Cong1, LIU Jinping2, LIU Jinsong1
Author information +
文章历史 +

摘要

目的 借助Gleeble-3500热模拟试验机进行热压缩实验,研究新型Ni-Cr-Fe基高温合金在变形温度为1 075~1 150 ℃、应变速率为0.001~1 s-1条件下的流变行为。方法 采用金相显微镜和透射电子显微镜观察合金热变形显微组织。构建了基于应变补偿的Arrhenius模型和BP网络模型。结果 新型Ni-Cr-Fe基高温合金流变应力受热变形参数的影响较为显著,与变形温度呈负相关,并与应变速率呈正相关。由显微组织分析可知,在1 150 ℃/0.01 s-1变形条件下,合金内部原始晶粒基本被细小的动态再结晶晶粒所取代。在0.1 s-1/ 1 075 ℃变形条件下,可以明显观察到大量位错缠结堆积在一起;同时还能观察到由于位错堆积和迁移而形成的位错墙。当应变速率降低至0.01 s-1时,晶粒内部位错密度显著降低且还能观察到动态再结晶晶核。利用2类模型预测了合金流变应力随应变的变化情况,其中BP神经网络模型的相关系数为0.998 5、平均相对误差为1.752 1%,预测精度较基于应变补偿的Arrhenius本构模型更高。结论 建立的BP神经网络模型更加适用于预测新型Ni-Cr-Fe基高温合金的流变应力。

Abstract

The work aims to study the hot deformation behavior of a novel Ni-Cr-Fe based superalloy in the temperature range of 1 075-1 150 ℃ and strain rate range of 0.001-1 s-1 by carrying out hot compression tests on a Gleeble-3500 thermo- mechanical simulator. Metallographic microscope and transmission electron microscope were used to observe hot deformation microstructure of the studied alloy. At the same time, the Arrhenius constitutive model based on strain compensation and BP (back-propagation) neural network model were also established. The flow stress of a novel Ni-Cr-Fe based superalloy was significantly affected by hot deformation parameters, which was negatively correlated with deformation temperature and positively correlated with strain rate. The microstructure analysis showed that the original grains inside the studied alloy were basically replaced by fine dynamic recrystallization (DRX) grains under the deformation condition of 1 150 ℃/0.01 s-1. Under the deformation condition of 0.1 s-1/1 075 ℃, a large number of dislocation tangles were clearly observed. At the same time, the dislocation wall formed by dislocation accumulation and migration was also observed. As the strain rate decreased to 0.01 s-1, it was found that the dislocation density inside the grains decreased significantly and the DRX nuclei was observed. Two kinds of models were used to predict the variation of flow stress with strain. The correlation coefficient of BP neural network model was 0.998 5 and the average relative error was 1.752 1%. The prediction accuracy of BP neural network model was higher than that of Arrhenius constitutive model based on strain compensation. The established BP neural network model is more suitable for accurately predicting the flow stress of a novel Ni-Cr-Fe based superalloy.

关键词

镍基高温合金 / 热变形 / 微观组织 / 本构模型 / 神经网络

Key words

nickel-based superalloy / hot deformation / microstructure / constitutive model / neural network

引用本文

导出引用
杜方鑫, 赵聪, 刘晋平, 刘劲松. 新型Ni-Cr-Fe基高温合金热变形行为研究[J]. 精密成形工程. 2025, 17(9): 176-184 https://doi.org/10.3969/j.issn.1674-6457.2025.09.017
DU Fangxin, ZHAO Cong, LIU Jinping, LIU Jinsong. Hot Deformation Behavior of a Novel Ni-Cr-Fe Based Superalloy[J]. Journal of Netshape Forming Engineering. 2025, 17(9): 176-184 https://doi.org/10.3969/j.issn.1674-6457.2025.09.017
中图分类号: TG302   

参考文献

[1] 杜占江, 丛相州, 孙立明, 等. 耐高温镍基合金管件制备工艺及组织性能[J]. 锻压技术, 2024, 49(8): 67-72.
DU Z J, CONG X Z, SUN L M, et al.Preparation Process and Microstructure Properties of High-Temperature Resistant Nickel-Based Alloy Pipe Fittings[J]. Forging & Stamping Technology, 2024, 49(8): 67-72.
[2] ZHENG W P, ZHU Y M, ZHANG Y, et al.Research on Heat Treatment of Nickel-Based Superalloys by Laser Powder Bed Fusion: A Review[J]. Journal of Alloys and Compounds, 2025, 1010: 177522.
[3] 罗阳, 张文云, 陈丽芳, 等. 某航空发动机用GH4065A合金低压涡轮盘锻件研制[J]. 铝加工, 2022(4): 64-68.
LUO Y, ZHANG W Y, CHEN L F, et al.Development of GH4065A Alloy Low Pressure Turbine Disk Forging for an Aeroengine[J]. Aluminium Fabrication, 2022(4): 64-68.
[4] CHATTREE A, PANDEY A, NENE S S, et al.High-Temperature Deformation Behavior and Concurrent Microstructural Evolution in Novel Ni-Based Compositionally Complex Alloy[J]. Journal of Alloys and Metallurgical Systems, 2024, 8: 100127.
[5] ZHAO P, WANG N, ZHANG P, et al.Dynamic Strain Ageing of Austenitic Ni-Based Alloy during Cyclic Loading at 350 ℃: Mechanism and Its Evolution[J]. Journal of Materials Research and Technology, 2024, 33: 4713-4724.
[6] ZHU H, OU H G.Constitutive Modelling of Hot Deformation Behaviour of Metallic Materials[J]. Materials Science and Engineering: A, 2022, 832: 142473.
[7] BROWN C, MCCARTHY T, CHADHA K, et al.Constitutive Modeling of the Hot Deformation Behavior of CoCrFeMnNi High-Entropy Alloy[J]. Materials Science and Engineering: A, 2021, 826: 141940.
[8] 姜炳春, 卢立伟, 文泽军, 等. LZ92镁锂合金流变应力预测模型[J]. 材料热处理学报, 2020, 41(9): 147-154.
JIANG B C, LU L W, WEN Z J, et al.Flow Stress Prediction Model of LZ92 Magnesium Lithium Alloy[J]. Transactions of Materials and Heat Treatment, 2020, 41(9): 147-154.
[9] 张开铭, 温余远, 王克鲁, 等. Ti-22Al-24Nb合金热变形行为及本构关系[J]. 塑性工程学报, 2022, 29(10): 208-215.
ZHANG K M, WEN Y Y, WANG K L, et al.Hot Deformation Behavior and Constitutive Relation of Ti-22Al-24Nb Alloy[J]. Journal of Plasticity Engineering, 2022, 29(10): 208-215.
[10] 朱大奇, 史慧. 人工神经网络原理及应用[M]. 北京: 科学出版社, 2006.
ZHU D Q, SHI H.Principle and Application of Artificial Neural Network[M]. Beijing: Science Press, 2006.
[11] 肖展开, 梅益, 罗宁康, 等. 基于神经网络航空发动机曲轴加工工艺设计优化[J]. 锻压技术, 2022, 47(6): 35-46.
XIAO Z K, MEI Y, LUO N K, et al.Design and Optimization on Machining Process for Aircraft Engine Crankshaft Based on Neural Network[J]. Forging & Stamping Technology, 2022, 47(6): 35-46.
[12] QIAO L, DENG Y, LIAO M Q, et al.Modelling and Prediction of Thermal Deformation Behaviors in a Pearlitic Steel[J]. Materials Today Communications, 2020, 25: 101134.
[13] BABU K, PRITHIV T S, GUPTA A, et al.Modeling and Simulation of Dynamic Recrystallization in Super Austenitic Stainless Steel Employing Combined Cellular Automaton, Artificial Neural Network and Finite Element Method[J]. Computational Materials Science, 2021, 195: 110482.
[14] 张韩旭, 方刚. 人工神经网络在金属塑性本构建模中的应用[J]. 锻压技术, 2024, 49(7): 1-18.
ZHANG H X, FANG G.Application of Artificial Neural Networks in Metal Plasticity Constitutive Modeling[J]. Forging & Stamping Technology, 2024, 49(7): 1-18.
[15] 左正, 郭淑玲, 张文文, 等. GH4698高温合金变形中的流变行为及显微组织[J]. 锻压技术, 2020, 45(1): 193-199.
ZUO Z, GUO S L, ZHANG W W, et al.Rheological Behavior and Microstructure of Super Alloy GH4698 during Deformation[J]. Forging & Stamping Technology, 2020, 45(1): 193-199.
[16] CHEN R C, ZHENG Z Z, LI J J, et al.Constitutive Modelling and Hot Workability Analysis by Microstructure Examination of GH4169 Alloy[J]. Crystals, 2018, 8(7): 282.
[17] ZHANG S Y, WANG J Z, HUANG L, et al.Correction of Flow Stress Data Due to Non-Homogeneous Deformation and Thermal Conditions during Hot Compression Testing of a Polycrystalline Nickel-Base Superalloy[J]. Journal of Materials Science, 2021, 56(12): 7727-7739.
[18] ZHONG M J, YU H, WANG Z R, et al.Hot Deformation Behavior and Process Parameters Optimization of GH4738 Nickel-Based Superalloy[J]. Journal of Materials Research and Technology, 2024, 33: 7990-8001.
[19] 高兴健, 刘鑫, 罗健, 等. DP1180钢的热变形Arrhenius本构模型[J]. 精密成形工程, 2024, 16(11): 108-116.
GAO X J, LIU X, LUO J, et al.Arrhenius Constitutive Model for Hot Deformation of DP1180 Steel[J]. Journal of Netshape Forming Engineering, 2024, 16(11): 108-116.
[20] ZYGUŁA K, LYPCHANSKYI O, CICHOCKI K, et al. Achieving High Density and Controlled Microstructure by Predicting Hot Deformation Behavior of Low-Cost Powder Metallurgy Ti-5553 Alloy[J]. Journal of Materials Research and Technology, 2024, 33: 8403-8424.
[21] 张兵, 刘鹏茹, 陈韩锋, 等. 铸态GH2132合金热变形行为和热加工图[J]. 中国有色金属学报, 2022, 32(2): 466-475.
ZHANG B, LIU P R, CHEN H F, et al.Thermal Deformation Behavior and Hot Processing Map of As-Cast GH2132 Alloy[J]. The Chinese Journal of Nonferrous Metals, 2022, 32(2): 466-475.
[22] 王岩, 谷宇, 王珏, 等. 铸态镍基高温合金GH4698热变形行为[J]. 锻压技术, 2021, 46(11): 250-254.
WANG Y, GU Y, WANG J, et al.Hot Deformation Behavior of As-Cast Ni-Based Superalloy GH4698[J]. Forging & Stamping Technology, 2021, 46(11): 250-254.
[23] 杨京, 王伟, 张双杰, 等. 15CrMoG耐热钢高温变形行为及Arrhenius本构模型[J]. 塑性工程学报, 2024, 31(2): 137-145.
YANG J, WANG W, ZHANG S J, et al.High-Temperature Deformation Behavior of 15CrMoG Heat-Resistant Steel and Arrhenius Constitutive Model[J]. Journal of Plasticity Engineering, 2024, 31(2): 137-145.
[24] GUO S, LIU C Y, LI R W, et al.A Hot Deformation Constitutive Model Applicable for Complete Austenite and Dynamic Ferrite Transformation Interval[J]. Materials Science and Engineering: A, 2024, 918: 147419.
[25] 冯瑞, 王克鲁, 鲁世强, 等. Zr-4合金热变形行为及物理本构模型[J]. 稀有金属材料与工程, 2021, 50(2): 525-530.
FENG R, WANG K L, LU S Q, et al.Hot Deformation Behavior and Strain Compensation Physical Constitutive Model of Zr-4 Alloy[J]. Rare Metal Materials and Engineering, 2021, 50(2): 525-530.
[26] YANG X W, LI W Y, MA J, et al.Thermo-Physical Simulation of the Compression Testing for Constitutive Modeling of GH4169 Superalloy during Linear Friction Welding[J]. Journal of Alloys and Compounds, 2016, 656: 395-407.
[27] 万鹏, 王克鲁, 鲁世强, 等. 基于应变补偿和PSO-BP神经网络的Ti-2.7Cu合金本构关系[J]. 材料工程, 2019, 47(4): 113-119.
WAN P, WANG K L, LU S Q, et al.Constitutive Modeling of Ti-2.7Cu Alloy Based on Strain Compensation and PSO-BP Neural Network[J]. Journal of Materials Engineering, 2019, 47(4): 113-119.
[28] REZAEI ASHTIANI H R, SHAYANPOOR A A. Hot Deformation Characterization of Pure Aluminum Using Artificial Neural Network (ANN) and Processing Map Considering Initial Grain Size[J]. Metals and Materials International, 2021, 27(12): 5017-5033.

基金

贵州省科技计划项目(黔科合基础-ZK[2024]重点062); 湖北省教育厅科技项目(B2018503); 武汉城市职业学院科研创新团队资助项目(2023whcvcTD02)

PDF(6913 KB)

Accesses

Citation

Detail

段落导航
相关文章

/